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The resulting reaction mixture was centrifuged at 15,000 g for 10 min, and the supernatant was analyzed by LC-FL (Waters, Milford, MA, USA) and LC-MS/MS (Shimazu, Kyoto, Japan)

, 11 , 239, doi: Shibata, Y., Yasui, H., Higashikawa, K., Miyamoto, N., and Kuge, Y